Colloids and Surfaces A 538 (2018) 1–6 Contents lists available at ScienceDirect Colloids and Surfaces A journal homepage: www.elsevier.com/locate/colsurfa Research Paper Low temperature synthesis of titanium oxide sol and gel with Nb doping using dialysis process of metal chloride solution Naofumi Uekawa , Eri Asano, Yugo Inagaki, Takashi Kojima Graduate School of Engineering, Chiba University, 1-33 Yayoi-cho, Inage-ku, Chiba-shi, Chiba, 263-8522 Japan GR APHICAL A BSTRACT ARTICLE I NFO ABSTRACT Keywords: Sol of layered titanate particles was obtained by stirring mixed solution of ethylene glycol and TiCl aq. at room Nb-doped TiO 2 temperature for 24 h and gel was obtained by dialysis of the obtained sol. According to XRD measurement, the Nanoparticle obtained gel consisted of anatase TiO nanoparticles. Metal chloride Synthesis of Nb-doped anatase TiO gel was also examined. Stirring the mixture of ethylene glycol, TiCl aq., 2 3 Gel and ethanol solution of NbCl also formed the layered titanate sol and Nb-doped anatase TiO gel was obtained 5 2 Dialysis by dialysis of the sol. Furthermore, heat treatment of the obtained gel was carried out by soaking it in H Oat 368 K for 24 h. This procedure greatly improved degree of crystallization of the anatase
Colloids and Surfaces A: Physicochemical and Engineering Aspects – Elsevier
Published: Feb 5, 2018
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