•A combination of in situ DRIFT and 2D-PCIS analysis was first used on pyrolysis.•Evolution of crystalline and amorphous cellulose during pyrolysis was explored.•H-bonds can rupture at a temperature >120 °C leading to free hydroxyls.•H-bonds in amorphous cellulose reduce more significantly.•Amorphous cellulose decomposes earlier due to the advanced saturated carbonyls.
Fuel – Elsevier
Published: Mar 15, 2018
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