Efficient preparation and comprehensive properties of thermal decomposition and detonation for 4,4′-dinitro-3,3′-azofuroxan

Efficient preparation and comprehensive properties of thermal decomposition and detonation for... •An efficient synthetic method with improved yield for preparing 4,4′-dinitro-3,3′-azofuroxan was developed.•The molecular structure of 4,4′-dinitro-3,3′-azofuroxan was confirmed by its crystal structure.•The detonation velocity of 4,4′-dinitro-3,3′-azofuroxan was determined by experiment.•The thermal behavior of 4,4′-dinitro-3,3′-azofuroxan was described.•The decomposition mechanism under heating and electron impact condition were proposed, respectively. http://www.deepdyve.com/assets/images/DeepDyve-Logo-lg.png Journal of Analytical and Applied Pyrolysis Elsevier

Efficient preparation and comprehensive properties of thermal decomposition and detonation for 4,4′-dinitro-3,3′-azofuroxan

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Publisher
Elsevier
Copyright
Copyright © 2017 Elsevier Ltd
ISSN
0165-2370
eISSN
1873-250X
D.O.I.
10.1016/j.jaap.2017.06.015
Publisher site
See Article on Publisher Site

Abstract

•An efficient synthetic method with improved yield for preparing 4,4′-dinitro-3,3′-azofuroxan was developed.•The molecular structure of 4,4′-dinitro-3,3′-azofuroxan was confirmed by its crystal structure.•The detonation velocity of 4,4′-dinitro-3,3′-azofuroxan was determined by experiment.•The thermal behavior of 4,4′-dinitro-3,3′-azofuroxan was described.•The decomposition mechanism under heating and electron impact condition were proposed, respectively.

Journal

Journal of Analytical and Applied PyrolysisElsevier

Published: Nov 1, 2017

References

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