Determination of dinitolmide and its metabolite 3-ANOT in chicken tissues via ASE-SPE-GC–MS/MS

Determination of dinitolmide and its metabolite 3-ANOT in chicken tissues via ASE-SPE-GC–MS/MS Journal of Food Composition and Analysis 71 (2018) 94–103 Contents lists available at ScienceDirect Journal of Food Composition and Analysis journal homepage: www.elsevier.com/locate/jfca Original research article Determination of dinitolmide and its metabolite 3-ANOT in chicken tissues via ASE-SPE-GC–MS/MS a,b,c a,b,c a,b,c, a,b,c a,b,c Xia Zhao , Bo Wang , Kaizhou Xie , Yanan Liu , Yangyang Zhang , a,b,c a,b,c a,b,c a,b,c a,b,c Yajuan Wang , Yawen Guo , Xiaona Bu , Chujun Liu , Genxi Zhang , a,b,c a,b,c Guojun Dai , Jinyu Wang College of Animal Science and Technology, Yangzhou University, Yangzhou 225009, China Key Laboratory for Animal Genetics, Breeding, Reproduction and Molecular Design of Jiangsu Province, Yangzhou 225009, China Joint International Research Laboratory of Agriculture and Agri-Product Safety, Yangzhou University, Yangzhou 225009, China ARTIC L E I NF O ABSTRAC T Keywords: A novel confirmatory analysis method to simultaneously extract, clean-up and detect dinitolmide and its me- Chicken tissues tabolite (3-amino-2-methyl-5-nitrobenzamide, 3-ANOT) in chicken tissues using accelerated solvent extraction Dinitolmide (ASE) with a neutral alumina solid-phase extraction (SPE) column coupled with gas chromatography-tandem 3-ANOT (3-amino-2-methyl-5-nitrobenzamide) mass spectrometry (ASE-SPE-GC–MS/MS) was established. GC–MS/MS was performed using a VF-5ht capillary GC–MS/MS column with helium as the carrier gas, temperature http://www.deepdyve.com/assets/images/DeepDyve-Logo-lg.png Journal of Food Composition and Analysis Elsevier

Determination of dinitolmide and its metabolite 3-ANOT in chicken tissues via ASE-SPE-GC–MS/MS

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Publisher
Elsevier
Copyright
Copyright © 2018 Elsevier Inc.
ISSN
0889-1575
D.O.I.
10.1016/j.jfca.2018.05.011
Publisher site
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Abstract

Journal of Food Composition and Analysis 71 (2018) 94–103 Contents lists available at ScienceDirect Journal of Food Composition and Analysis journal homepage: www.elsevier.com/locate/jfca Original research article Determination of dinitolmide and its metabolite 3-ANOT in chicken tissues via ASE-SPE-GC–MS/MS a,b,c a,b,c a,b,c, a,b,c a,b,c Xia Zhao , Bo Wang , Kaizhou Xie , Yanan Liu , Yangyang Zhang , a,b,c a,b,c a,b,c a,b,c a,b,c Yajuan Wang , Yawen Guo , Xiaona Bu , Chujun Liu , Genxi Zhang , a,b,c a,b,c Guojun Dai , Jinyu Wang College of Animal Science and Technology, Yangzhou University, Yangzhou 225009, China Key Laboratory for Animal Genetics, Breeding, Reproduction and Molecular Design of Jiangsu Province, Yangzhou 225009, China Joint International Research Laboratory of Agriculture and Agri-Product Safety, Yangzhou University, Yangzhou 225009, China ARTIC L E I NF O ABSTRAC T Keywords: A novel confirmatory analysis method to simultaneously extract, clean-up and detect dinitolmide and its me- Chicken tissues tabolite (3-amino-2-methyl-5-nitrobenzamide, 3-ANOT) in chicken tissues using accelerated solvent extraction Dinitolmide (ASE) with a neutral alumina solid-phase extraction (SPE) column coupled with gas chromatography-tandem 3-ANOT (3-amino-2-methyl-5-nitrobenzamide) mass spectrometry (ASE-SPE-GC–MS/MS) was established. GC–MS/MS was performed using a VF-5ht capillary GC–MS/MS column with helium as the carrier gas, temperature

Journal

Journal of Food Composition and AnalysisElsevier

Published: Aug 1, 2018

References

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