Journal of Food Composition and Analysis 71 (2018) 94–103 Contents lists available at ScienceDirect Journal of Food Composition and Analysis journal homepage: www.elsevier.com/locate/jfca Original research article Determination of dinitolmide and its metabolite 3-ANOT in chicken tissues via ASE-SPE-GC–MS/MS a,b,c a,b,c a,b,c, a,b,c a,b,c Xia Zhao , Bo Wang , Kaizhou Xie , Yanan Liu , Yangyang Zhang , a,b,c a,b,c a,b,c a,b,c a,b,c Yajuan Wang , Yawen Guo , Xiaona Bu , Chujun Liu , Genxi Zhang , a,b,c a,b,c Guojun Dai , Jinyu Wang College of Animal Science and Technology, Yangzhou University, Yangzhou 225009, China Key Laboratory for Animal Genetics, Breeding, Reproduction and Molecular Design of Jiangsu Province, Yangzhou 225009, China Joint International Research Laboratory of Agriculture and Agri-Product Safety, Yangzhou University, Yangzhou 225009, China ARTIC L E I NF O ABSTRAC T Keywords: A novel conﬁrmatory analysis method to simultaneously extract, clean-up and detect dinitolmide and its me- Chicken tissues tabolite (3-amino-2-methyl-5-nitrobenzamide, 3-ANOT) in chicken tissues using accelerated solvent extraction Dinitolmide (ASE) with a neutral alumina solid-phase extraction (SPE) column coupled with gas chromatography-tandem 3-ANOT (3-amino-2-methyl-5-nitrobenzamide) mass spectrometry (ASE-SPE-GC–MS/MS) was established. GC–MS/MS was performed using a VF-5ht capillary GC–MS/MS column with helium as the carrier gas, temperature
Journal of Food Composition and Analysis – Elsevier
Published: Aug 1, 2018
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