Are nanojars unique to copper? Solution and solid state characterization of high-symmetry octanuclear nickel(II)-pyrazolate complexes

Are nanojars unique to copper? Solution and solid state characterization of high-symmetry... Inorganica Chimica Acta 475 (2018) 65–72 Contents lists available at ScienceDirect Inorganica Chimica Acta journal homepage: www.elsevier.com/locate/ica Are nanojars unique to copper? Solution and solid state characterization of high-symmetry octanuclear nickel(II)-pyrazolate complexes Wisam A. Al Isawi, Basil M. Ahmed, Christian K. Hartman, Alexandria N. Seybold, Gellert Mezei Department of Chemistry, Western Michigan University, Kalamazoo, MI, USA article i nfo abstract Article history: A comprehensive study using sixteen different metal ions was conducted, in order to test the possibility 2+ 2 2 Received 21 June 2017 of substituting one or more Cu ions in nanojars, [anion{Cu(l-OH)(l-pz)} ] (n = 27–32; anion = CO n 3 Received in revised form 31 July 2017 2 2+ 2+ 2+ 2+ 3+ 2+ 3+ 2+ 2+ + 2+ 4+ 2+ 2+ 3+ 3+ or SO ), with Zn ,Ni ,Co ,Fe ,Fe ,Mn ,Cr ,VO ,Cd ,Ag ,Pd ,Ce ,Sn ,Pb ,Pr or Nd .An Accepted 3 August 2017 2+ octanuclear nickel complex was isolated in the case of Ni , which inspired the synthesis of a series of Available online 9 August 2017 (Bu N) [Ni (l -OH) (l-4-Rpz) ] (R = H, Me, Oct) complexes. Characterization was carried out in the 4 http://www.deepdyve.com/assets/images/DeepDyve-Logo-lg.png Inorganica Chimica Acta Elsevier

Are nanojars unique to copper? Solution and solid state characterization of high-symmetry octanuclear nickel(II)-pyrazolate complexes

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Publisher
Elsevier
Copyright
Copyright © 2017 Elsevier B.V.
ISSN
0020-1693
eISSN
1873-3255
D.O.I.
10.1016/j.ica.2017.08.013
Publisher site
See Article on Publisher Site

Abstract

Inorganica Chimica Acta 475 (2018) 65–72 Contents lists available at ScienceDirect Inorganica Chimica Acta journal homepage: www.elsevier.com/locate/ica Are nanojars unique to copper? Solution and solid state characterization of high-symmetry octanuclear nickel(II)-pyrazolate complexes Wisam A. Al Isawi, Basil M. Ahmed, Christian K. Hartman, Alexandria N. Seybold, Gellert Mezei Department of Chemistry, Western Michigan University, Kalamazoo, MI, USA article i nfo abstract Article history: A comprehensive study using sixteen different metal ions was conducted, in order to test the possibility 2+ 2 2 Received 21 June 2017 of substituting one or more Cu ions in nanojars, [anion{Cu(l-OH)(l-pz)} ] (n = 27–32; anion = CO n 3 Received in revised form 31 July 2017 2 2+ 2+ 2+ 2+ 3+ 2+ 3+ 2+ 2+ + 2+ 4+ 2+ 2+ 3+ 3+ or SO ), with Zn ,Ni ,Co ,Fe ,Fe ,Mn ,Cr ,VO ,Cd ,Ag ,Pd ,Ce ,Sn ,Pb ,Pr or Nd .An Accepted 3 August 2017 2+ octanuclear nickel complex was isolated in the case of Ni , which inspired the synthesis of a series of Available online 9 August 2017 (Bu N) [Ni (l -OH) (l-4-Rpz) ] (R = H, Me, Oct) complexes. Characterization was carried out in the 4

Journal

Inorganica Chimica ActaElsevier

Published: Apr 24, 2018

References

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