Application of quantitative inline NMR spectroscopy for investigation of a fixed-bed chromatographic reactor process

Application of quantitative inline NMR spectroscopy for investigation of a fixed-bed... Chemical Engineering Journal 336 (2018) 518–530 Contents lists available at ScienceDirect Chemical Engineering Journal journal homepage: www.elsevier.com/locate/cej Application of quantitative inline NMR spectroscopy for investigation of a fixed-bed chromatographic reactor process a b c,d c,e Alexander Brächer , Lisa Maria Kreußer , Shamsul Qamar , Andreas Seidel-Morgenstern , a, Erik von Harbou Laboratory of Engineering Thermodynamics, University of Kaiserslautern, Erwin-Schrödinger-Straße 44, 67663 Kaiserslautern, Germany Department of Applied Mathematics and Theoretical Physics, Centre for Mathematical Sciences, Wilberforce Road, Cambridge CB3 0WA, United Kingdom Max Planck Institute (MPI) for Dynamics of Complex Technical Systems, Sandtorstraße 1, 39106 Magdeburg, Germany Department of Mathematics, COMSATS Institute of Information Technology, Park Road, Chak Shahzad, Islamabad, Pakistan Otto-von-Guericke-Universität, Institut für Verfahrenstechnik, Universitätsplatz 2, 39106 Magdeburg, Germany GR APHICAL A BSTRACT ARTICLE I NFO ABSTRACT Keywords: A Nuclear Magnetic Resonance (NMR) spectroscopy method is presented that facilitates inline analysis of dy- Fixed-bed chromatographic reactor namic processes. Compared to other commonly used optical inline analysis methods, NMR spectroscopy has the Inline NMR spectroscopy advantage that it can resolve different species in complex multicomponent mixtures. An inline NMR spectro- Dynamic process scopy method was optimized to enable analysis with high temporal resolution. The method was applied to study http://www.deepdyve.com/assets/images/DeepDyve-Logo-lg.png Chemical Engineering Journal Elsevier

Application of quantitative inline NMR spectroscopy for investigation of a fixed-bed chromatographic reactor process

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Publisher
Elsevier
Copyright
Copyright © 2017 Elsevier B.V.
ISSN
1385-8947
eISSN
1873-3212
D.O.I.
10.1016/j.cej.2017.12.004
Publisher site
See Article on Publisher Site

Abstract

Chemical Engineering Journal 336 (2018) 518–530 Contents lists available at ScienceDirect Chemical Engineering Journal journal homepage: www.elsevier.com/locate/cej Application of quantitative inline NMR spectroscopy for investigation of a fixed-bed chromatographic reactor process a b c,d c,e Alexander Brächer , Lisa Maria Kreußer , Shamsul Qamar , Andreas Seidel-Morgenstern , a, Erik von Harbou Laboratory of Engineering Thermodynamics, University of Kaiserslautern, Erwin-Schrödinger-Straße 44, 67663 Kaiserslautern, Germany Department of Applied Mathematics and Theoretical Physics, Centre for Mathematical Sciences, Wilberforce Road, Cambridge CB3 0WA, United Kingdom Max Planck Institute (MPI) for Dynamics of Complex Technical Systems, Sandtorstraße 1, 39106 Magdeburg, Germany Department of Mathematics, COMSATS Institute of Information Technology, Park Road, Chak Shahzad, Islamabad, Pakistan Otto-von-Guericke-Universität, Institut für Verfahrenstechnik, Universitätsplatz 2, 39106 Magdeburg, Germany GR APHICAL A BSTRACT ARTICLE I NFO ABSTRACT Keywords: A Nuclear Magnetic Resonance (NMR) spectroscopy method is presented that facilitates inline analysis of dy- Fixed-bed chromatographic reactor namic processes. Compared to other commonly used optical inline analysis methods, NMR spectroscopy has the Inline NMR spectroscopy advantage that it can resolve different species in complex multicomponent mixtures. An inline NMR spectro- Dynamic process scopy method was optimized to enable analysis with high temporal resolution. The method was applied to study

Journal

Chemical Engineering JournalElsevier

Published: Mar 15, 2018

References

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