Journal of Colloid and Interface Science 461 (2016) 173–178 Contents lists available at ScienceDirect Journal of Colloid and Interface Science journal homepage: www.elsevier.com/locate/jcis A facile synthesis of superparamagnetic Fe O supraparticles@MIL-100 3 4 (Fe) core–shell nanostructures: Preparation, characterization and biocompatibility Shoushan Yu, Jiaqi Wan, Kezheng Chen Laboratory of Functional and Biomedical Nanomaterials, College of Materials Science and Engineering, Qingdao University of Science and Technology, Qingdao 266042, PR China graphical a bstract article i nfo abstract Article history: Superparamagnetic Fe O supraparticles@MIL-100(Fe) core–shell nanostructure microspheres were suc- 3 4 Received 16 July 2015 cessfully constructed by a facile step-by-step method. The polyacrylate formed in situ during the process Revised 3 September 2015 of the preparation of Fe O supraparticles not only acted as a stabilizer on the Fe O nanoparticles sur- 3 4 3 4 Accepted 6 September 2015 face, but also played a crucial role as a ‘‘bridge” in the initial stage of the framework components selec- Available online 7 September 2015 tively assembly on the Fe O supraparticle surfaces. The structure and composition of the obtained 3 4 microspheres were characterized by SEM, TEM, DLS, XRD, FTIR, and TG analysis. The MPMS results Keywords: revealed that the introduction
Journal of Colloid and Interface Science – Elsevier
Published: Jan 1, 2016
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