Zeitschrift für © by R. Kristallographie 205, 117-118 (1993) Oldenbourg Verlag, München 1993 0044-2968/93 $3.00 + 0.00 Crystal structure refinement of dineodymium(III) dioxide Institut für monosulfide, Nd202S W-3000 Hannover 1 F. Lissner and Th. Schleid Anorganische Chemie der Universität Hannover, Callinstr. 9, to database ICSD (Received May 14, 1992, transferred September 30, 1992) Source of material: see refs. 7 and 8. Trigonal, P3ml (no 164), 3.9498(3), 6.7920(8) Â, 91.8Â3, l, Table t. Parameters used for the F. Lissner and Th. Schleid X-ray data collection Number of unique reflections: 255 Criterion for unobserved reflections: F,, < 2ct(F,,) Number of refined 10 parameters: Scan mode : 20-scan 284.57 cm"1 µ; Structure solution SHELX program used: Diffractometcr type: Wavelength: Crystal characteristics: Sicmens-Stoe AED2 Mo K, radiation (.71073 triangular platelet, light blue, transparent, size mm Â) Temperature of measurement: 2Ömai: Table 2. Final atomic coordinates and Atom Nd displacement parameters (in Â2) U¡.,,Un U,, U,, 0.0061(2 ) U,2 0.00502(6 ) U,., U,., 0.27989(6 ) 0.6272(9) 0.0100(11 0.0100(1) 0.012(1) 0.0133(6) 0.012(1) 0.0133(6) 0.010(2) 0.0062(9) 0.0060(6) 0.0066(3) Further details of the structure determination (e.g. structure factors) have been deposited within the relevant database and can be accessed as Collection No. 300245 or ordered from
Zeitschrift für Kristallographie - Crystalline Materials – de Gruyter
Published: Jan 1, 1993
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