Zeitschrift für Kristallographie 205, 146- 148 (1993) © by R. Oldenbourg Verlag, München 1993 0044-2968/93 $3.00 + 0.00 Crystal structure of N-(2-hydroxyphenyl)salicylaldiminato-pyridine-copper(II), (0(C6H4)CHN(C6H4)0(NC5H5)Cu) A. Elmali Department of Engineering Physics, Faculty of Sciences, University of Ankara, 06100 Besevler Ankara, Turkey and O. Atakol Department of Chemistry, Faculty of Sciences, University of Ankara, 06100 Besevler Turkey and I. Svoboda and H. Fuess Ankara, Strukturforschung, FB Materialwissenschaft, Technische Hochschule Darmstadt, Petersenstr. 20, W-6100 Darmstadt (Received July 3, 1992) Source of material: Reaction of N-(2-hydroxyphenyl)-salicylaldimine with Pyridine in propanol solution and a methanolic solution of Cu(OAc)2 H20. Hydrogen H(l) for C(l) and C(1A) determined by difference fourier. The other hydrogen atoms were geometrically positioned at a C- distance of 0.98 A. N-(2-hydroxyphenyl)-salicylaldiminato-pyridine-copper(II) Orthorhombic, Pna2, (no 33), Â3, 4, R 9.834(4), b 11.431(3), 13.425(3) Â, V Table 1. Parameters used for the Diffractometer X-ray data collection Number of unique reflections: 1255 Criterion for unobserved reflections: F,, < 4a(F0) Number of refined 209 parameters: Scan mode: µ: 14.30 cm-1 type: Wave length: characteristics: Temperature of measurement : Crystal dark green needle, size 0.65x0.2x0.2 mm 300 50° (0.7107 Â) Enraf-Nonius CAD4 Mo K, radiation /20 "mai Structure solution program used: SHELX Table 2. Final atomic
Zeitschrift für Kristallographie - Crystalline Materials – de Gruyter
Published: Jan 1, 1993
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