Zeitschrift für Kristallographie 206, 141 142 (1993) © by R. Oldenbourg Verlag, München 1993 0044-2968/93 $3.00 Crystal structure of hexapotassium triarsenidoindate, K6I11AS3 W. Blase and G. Cordier Eduard-Zintl-Institut der Technischen Hochschule Dannstadt, Hochschulstr. 10, 6100 Darmstadt, Germany and M. Somer Max-Planck-Institut für Festkörperforschung, Heisenbergstr. 1, 7000 Stuttgart 80, Germany (Received October 5, 1992, transferred to database ICSD November 15, 1992) In As Source of material: Synthesis from the elements at 870 K in sealed Nb-ampoules. The In atoms are slightly distorted trigonal planar coordinated by As atoms (In-As: 2.605(2) 2.623(2) Â). The [InAs3]6" anion is isostructural to [B03r Triclinic, PÏ (No. 2), a ß 94.5(1)°, y 9.130(2) k,b = 9.112(2) Â, c 19.609(5) Â, 119.9(1)°, V 1398.6 Â3, Z 4, R 0.062. = = = = 94.2(1)°, Table 1. Parameters used for the Diffractometer W. Blase, G. Cordier and M. Somer X-ray data collection Number of unique reflections: Criterion for unobserved reflections: Philips PW1100 Mo K0. radiation type: Wave length: (0.7107 Â) F0 < 3 o-(Fo) Crystal characteristics: metallic lustrous, thin x 0.1 0.01 mm platelets, size 0.1 293 K 60° Number of refined parameters: Scan mode: Temperature of measurement: 6/26 cm"1 20max- Structure solution program used: SHELX
Zeitschrift für Kristallographie - Crystalline Materials – de Gruyter
Published: Jan 1, 1993
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