Crystal structure of dicaesium pentachlorothallate, Cs 2 TlCl 5

Crystal structure of dicaesium pentachlorothallate, Cs 2 TlCl 5 Zeitschrift für Kristallographie 205, 131-132 (1993) © by R. Oldenbourg Verlag, München 1993 0044-2968/93 $3.00 + 0.00 G. Thiele and R. Richter Institut für Anorganische und Analytische Chemie, Albertstr. 21, W-7800 Freiburg i. 27, 1992, transferred to database ICSD Br. (Received March September 30, 1992) ZI Crystallization from aqueous solutions of T1C13 and CsCl réf. 1). (see Distorted octahedral T1C16 groups (d(Tl-Cl) 2.50 -2.80 Â) are linked by common vertices to chain anions. Coordination number 10 for Cs. Source of material: Orthorhombic, Pnma (no 62), 1039.7 Â3, 4, R .031. = = 9.337(2), b 7.493(1), 14,861(3) Â, Table I. Parameters used for the G. Thiele and R. Richter X-ray data collection Number of unique reflections: 985 Criterion for unob< 4 ( 0) served reflections: Number of refined 46 parameters: Scan mode: 20-scan 237.8 cm-1 µ: Structure solution program used: SHELXTL-plus Diffractometer type: Wave length : Enraf-Nonius CAD4 Mo Ka radiation colourless needle, size 0.01 xO.l xO.01 mm Crystal characteristics: Temperature of measurement: (.71073 A) 20 "max ^· Table 2. Final atomic coordinates and displacement parameters (in Â2) U¡,,/U,, u2 0.0209(3) 0.0350(6) 0.0362(7) 0.037(2) 0.029(1) 0.040(2) 0.044(3) 0.0215(3) 0.0260(5) 0.0464(7) 0.034(2) 0.051(2) 0.035(2) 0.025(2) Ui3 -0.0010(2) 0.0 -0.0016(4) 0.0 http://www.deepdyve.com/assets/images/DeepDyve-Logo-lg.png Zeitschrift für Kristallographie - Crystalline Materials de Gruyter

Crystal structure of dicaesium pentachlorothallate, Cs 2 TlCl 5

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Publisher
de Gruyter
Copyright
Copyright © 1993 by the
ISSN
2194-4946
eISSN
2196-7105
DOI
10.1524/zkri.1993.205.Part-1.131
Publisher site
See Article on Publisher Site

Abstract

Zeitschrift für Kristallographie 205, 131-132 (1993) © by R. Oldenbourg Verlag, München 1993 0044-2968/93 $3.00 + 0.00 G. Thiele and R. Richter Institut für Anorganische und Analytische Chemie, Albertstr. 21, W-7800 Freiburg i. 27, 1992, transferred to database ICSD Br. (Received March September 30, 1992) ZI Crystallization from aqueous solutions of T1C13 and CsCl réf. 1). (see Distorted octahedral T1C16 groups (d(Tl-Cl) 2.50 -2.80 Â) are linked by common vertices to chain anions. Coordination number 10 for Cs. Source of material: Orthorhombic, Pnma (no 62), 1039.7 Â3, 4, R .031. = = 9.337(2), b 7.493(1), 14,861(3) Â, Table I. Parameters used for the G. Thiele and R. Richter X-ray data collection Number of unique reflections: 985 Criterion for unob< 4 ( 0) served reflections: Number of refined 46 parameters: Scan mode: 20-scan 237.8 cm-1 µ: Structure solution program used: SHELXTL-plus Diffractometer type: Wave length : Enraf-Nonius CAD4 Mo Ka radiation colourless needle, size 0.01 xO.l xO.01 mm Crystal characteristics: Temperature of measurement: (.71073 A) 20 "max ^· Table 2. Final atomic coordinates and displacement parameters (in Â2) U¡,,/U,, u2 0.0209(3) 0.0350(6) 0.0362(7) 0.037(2) 0.029(1) 0.040(2) 0.044(3) 0.0215(3) 0.0260(5) 0.0464(7) 0.034(2) 0.051(2) 0.035(2) 0.025(2) Ui3 -0.0010(2) 0.0 -0.0016(4) 0.0

Journal

Zeitschrift für Kristallographie - Crystalline Materialsde Gruyter

Published: Jan 1, 1993

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