Crystal structure of 6,12-diphenyl-1(4-tolyl)-11-azatetracyclo(4.4.2.0 2,5 .0 7,10 )dodeca-3,8,11-triene, (C 4 H 4 )CNCC(C 4 H 4 )(C 6 H 4 CH 3 )(C 6 H 5 ) 2

Crystal structure of 6,12-diphenyl-1(4-tolyl)-11-azatetracyclo(4.4.2.0 2,5 .0 7,10... Kristallographie 205, 151 -153 (1993) © by R. Oldenbourg Verlag, München 1993 0044-2968/93 $3.00 + 0.00 Zeitschrift für tetracyclo[4.4.2.02'5.0710]dodeca-3,8,ll-triene, (C4H4)CNCC(C4H4)(C6H4CH3)(C6H5)2 M. Crystal structure of 6,12-diphenyl-l(4-tolyl)-ll-aza- Vey, H. Neunhoeffer, S. Foro and H.-J. Lindner 22, Institut für Organische Chemie, Technische Hochschule Darmstadt, Petersenstr. W-6100 Darmstadt and H. Paulus and I. Svoboda FB Materialwissenschaft, FG Strukturforschung, Technische Hochschule Petersenstr. 20, W-6100 Darmstadt Darmstadt, (Received June 2, 1992) Source of material: (4-tolyl)-19-aza-octacyclo[8.8.2.24'7.213-16.02'9.03'8.0n'18.012'17]tetracosa-5,14, All Preparation by vacuum-pyrolysis of 10,20-diphenyl-l- 19,21,23-pentaene-5,6,14,15-tetracarboxylic acid tetramethylester hydrogen atoms are geometrically positioned. Orthorhombic, Pbca (no 61), a V 4464.4 A3, 8, R 0.049. = = = 23.262(8), 6= 16.559(5), 11.590(4) Â, M. Vey, H. Neunhoeffer, S. Foro, H.-J. Lindner, H. Paulus and I. Svoboda Table 1. Parameters used for the X-ray data collection Number of unique reflections : 2077 Criterion for unob< 2 ( 0) served reflections: Number of refined 285 parameters: Scan mode: 2/ 0.35 cm-1 µ: Structure solution SHELX program used : Diffractometer type: Wave length: Crystal characteristics: Temperature of measurement: colourless slab, size 0.22x0.51 1.00 mm 293 40° (0.7107 Â) Stoe-Stadi 4 Mo K, radiation 20max: Table 2. Final atomic coordinates and Atom displacement parameters (in Á2) UWU, U33 0.054(2) 0.056(2) 0.049(2) 0.048(2) 0.059(2) http://www.deepdyve.com/assets/images/DeepDyve-Logo-lg.png Zeitschrift für Kristallographie - Crystalline Materials de Gruyter

Crystal structure of 6,12-diphenyl-1(4-tolyl)-11-azatetracyclo(4.4.2.0 2,5 .0 7,10 )dodeca-3,8,11-triene, (C 4 H 4 )CNCC(C 4 H 4 )(C 6 H 4 CH 3 )(C 6 H 5 ) 2

Loading next page...
 
/lp/de-gruyter/crystal-structure-of-6-12-diphenyl-1-4-tolyl-11-azatetracyclo-4-4-2-0-qS7U5qDIXq
Publisher
de Gruyter
Copyright
Copyright © 1993 by the
ISSN
2194-4946
eISSN
2196-7105
DOI
10.1524/zkri.1993.205.Part-1.151
Publisher site
See Article on Publisher Site

Abstract

Kristallographie 205, 151 -153 (1993) © by R. Oldenbourg Verlag, München 1993 0044-2968/93 $3.00 + 0.00 Zeitschrift für tetracyclo[4.4.2.02'5.0710]dodeca-3,8,ll-triene, (C4H4)CNCC(C4H4)(C6H4CH3)(C6H5)2 M. Crystal structure of 6,12-diphenyl-l(4-tolyl)-ll-aza- Vey, H. Neunhoeffer, S. Foro and H.-J. Lindner 22, Institut für Organische Chemie, Technische Hochschule Darmstadt, Petersenstr. W-6100 Darmstadt and H. Paulus and I. Svoboda FB Materialwissenschaft, FG Strukturforschung, Technische Hochschule Petersenstr. 20, W-6100 Darmstadt Darmstadt, (Received June 2, 1992) Source of material: (4-tolyl)-19-aza-octacyclo[8.8.2.24'7.213-16.02'9.03'8.0n'18.012'17]tetracosa-5,14, All Preparation by vacuum-pyrolysis of 10,20-diphenyl-l- 19,21,23-pentaene-5,6,14,15-tetracarboxylic acid tetramethylester hydrogen atoms are geometrically positioned. Orthorhombic, Pbca (no 61), a V 4464.4 A3, 8, R 0.049. = = = 23.262(8), 6= 16.559(5), 11.590(4) Â, M. Vey, H. Neunhoeffer, S. Foro, H.-J. Lindner, H. Paulus and I. Svoboda Table 1. Parameters used for the X-ray data collection Number of unique reflections : 2077 Criterion for unob< 2 ( 0) served reflections: Number of refined 285 parameters: Scan mode: 2/ 0.35 cm-1 µ: Structure solution SHELX program used : Diffractometer type: Wave length: Crystal characteristics: Temperature of measurement: colourless slab, size 0.22x0.51 1.00 mm 293 40° (0.7107 Â) Stoe-Stadi 4 Mo K, radiation 20max: Table 2. Final atomic coordinates and Atom displacement parameters (in Á2) UWU, U33 0.054(2) 0.056(2) 0.049(2) 0.048(2) 0.059(2)

Journal

Zeitschrift für Kristallographie - Crystalline Materialsde Gruyter

Published: Jan 1, 1993

There are no references for this article.

You’re reading a free preview. Subscribe to read the entire article.


DeepDyve is your
personal research library

It’s your single place to instantly
discover and read the research
that matters to you.

Enjoy affordable access to
over 18 million articles from more than
15,000 peer-reviewed journals.

All for just $49/month

Explore the DeepDyve Library

Search

Query the DeepDyve database, plus search all of PubMed and Google Scholar seamlessly

Organize

Save any article or search result from DeepDyve, PubMed, and Google Scholar... all in one place.

Access

Get unlimited, online access to over 18 million full-text articles from more than 15,000 scientific journals.

Your journals are on DeepDyve

Read from thousands of the leading scholarly journals from SpringerNature, Wiley-Blackwell, Oxford University Press and more.

All the latest content is available, no embargo periods.

See the journals in your area

DeepDyve

Freelancer

DeepDyve

Pro

Price

FREE

$49/month
$360/year

Save searches from
Google Scholar,
PubMed

Create folders to
organize your research

Export folders, citations

Read DeepDyve articles

Abstract access only

Unlimited access to over
18 million full-text articles

Print

20 pages / month

PDF Discount

20% off