Crystal structure of 1,3-bis(1-methylbenzimidazol-2-yl)propane(acetonitrile)copper(I)hexafluorophosphate, Cu(C 19 H 20 N 4 )(CH 3 CN)(PF 6 )

Crystal structure of... Zeitschrift für Kristallographie 203, 135-137 © by R. Oldenbourg Verlag, München 1993 (1993) 0044-2968/93 $3.00 + 0.00 Crystal structure of l,3-bis(l-methylbenziniidazol-2-yl)propane(acetonitrile)copper(I)hexafluorophosphate, Cu(C19H20N4)(CH3CN)(PF6) G. Bernardinelli Laboratoire de Cristallographie, 24 quai Ernest-Ansermet, CH-1211 Geneva, Switzerland and A. Kubel-Pollak, S. Ruttimann and A. F. Williams Departement de Chimie Minerale, Analytique et Appliquée, CH-1211 Geneva, Switzerland (Received February 14, 1992) quai Ernest-Ansermet, Source of material : see ref. 1. = = Triclinic, Pi (no 2), a 7.5373(8), b 12.357(1), c 14.286(2) , 2, R 0.069. ß 75.75(1)°, 82.335(7)°, V 1169.7 Â3, = = = = 65.178(9)°, G. Bernardinelli, A. Kubel-Pollak, S. Ruttimann and A. X-ray data collection Number of unique reflections: 2425 Criterion for unobserved reflections : F,, < 4a(F0) Number of refined 310 parameters : Scan mode : co-2<9-scan 10.67 cm"1 µ: Structure solution Multan 87 XTAL3.0 program used : F. Williams Table 1. Parameters used for the Diffractometer type: Wave length: Philips PW1100 Mo K,, radiation Crystal characteristics : Temperature of measurement: colourless prism, size 0.10x0.17x0.28 mm 298 46° (0.7107 Â) 20 ''max Table 2. Final atomic coordinates and Atom displacement parameters (in Â2) u. u. Vl2 0.0069(4) -0.002(3) -0.008(4) 0.001(3) -0.001(3) -0.009(4) -0.013(4) -0.007(4) -0.018(5) -0.036(7) -0.050(8) -0.021(5) -0.011(6) http://www.deepdyve.com/assets/images/DeepDyve-Logo-lg.png Zeitschrift für Kristallographie - Crystalline Materials de Gruyter

Crystal structure of 1,3-bis(1-methylbenzimidazol-2-yl)propane(acetonitrile)copper(I)hexafluorophosphate, Cu(C 19 H 20 N 4 )(CH 3 CN)(PF 6 )

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Publisher
de Gruyter
Copyright
Copyright © 1993 by the
ISSN
2194-4946
eISSN
2196-7105
DOI
10.1524/zkri.1993.203.Part-1.135
Publisher site
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Abstract

Zeitschrift für Kristallographie 203, 135-137 © by R. Oldenbourg Verlag, München 1993 (1993) 0044-2968/93 $3.00 + 0.00 Crystal structure of l,3-bis(l-methylbenziniidazol-2-yl)propane(acetonitrile)copper(I)hexafluorophosphate, Cu(C19H20N4)(CH3CN)(PF6) G. Bernardinelli Laboratoire de Cristallographie, 24 quai Ernest-Ansermet, CH-1211 Geneva, Switzerland and A. Kubel-Pollak, S. Ruttimann and A. F. Williams Departement de Chimie Minerale, Analytique et Appliquée, CH-1211 Geneva, Switzerland (Received February 14, 1992) quai Ernest-Ansermet, Source of material : see ref. 1. = = Triclinic, Pi (no 2), a 7.5373(8), b 12.357(1), c 14.286(2) , 2, R 0.069. ß 75.75(1)°, 82.335(7)°, V 1169.7 Â3, = = = = 65.178(9)°, G. Bernardinelli, A. Kubel-Pollak, S. Ruttimann and A. X-ray data collection Number of unique reflections: 2425 Criterion for unobserved reflections : F,, < 4a(F0) Number of refined 310 parameters : Scan mode : co-2<9-scan 10.67 cm"1 µ: Structure solution Multan 87 XTAL3.0 program used : F. Williams Table 1. Parameters used for the Diffractometer type: Wave length: Philips PW1100 Mo K,, radiation Crystal characteristics : Temperature of measurement: colourless prism, size 0.10x0.17x0.28 mm 298 46° (0.7107 Â) 20 ''max Table 2. Final atomic coordinates and Atom displacement parameters (in Â2) u. u. Vl2 0.0069(4) -0.002(3) -0.008(4) 0.001(3) -0.001(3) -0.009(4) -0.013(4) -0.007(4) -0.018(5) -0.036(7) -0.050(8) -0.021(5) -0.011(6)

Journal

Zeitschrift für Kristallographie - Crystalline Materialsde Gruyter

Published: Jan 1, 1993

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