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We report the neutral-ionic transformation of N 2 ∕ O 2 mixtures above 5 GPa at 300 K . The reaction is photoinduced with a Nd:YAG laser irradiation. The ionic compounds are characterized by Raman and infrared spectroscopic and synchrotron x-ray diffraction measurements. We show by Raman analysis that the N O + N O 3 − compound can trap a large fraction of O 2 molecules, thus forming an O 2 clathrate. But no N 2 molecule can be included in this nitrosonium nitrate compound. We propose an orthorhombic unit cell with 10 N O + N O 3 − in it.
Physical Review B – American Physical Society (APS)
Published: Aug 1, 2006
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