TY - JOUR
AU - Rouilly, Antoine
AB - Cellulose (2019) 26:2941–2954 https://doi.org/10.1007/s10570-019-02273-8(0123456789().,-volV)(0123456789().,-volV) OR IGINAL RESEARCH Cellulose consolidation under high-pressure and high- temperature uniaxial compression . . . . Thibaud Pintiaux Maelie Heuls Virginie Vandenbossche Timothy Murphy . . . Richard Wuhrer Patrice Castignolles Marianne Gaborieau Antoine Rouilly Received: 14 August 2018 / Accepted: 17 January 2019 / Published online: 28 January 2019 Springer Nature B.V. 2019 Abstract Materials based on cellulose cannot be above the glass transition temperature was responsible obtained from thermoplastic processes. Our aim is to for water migration towards the specimen heart. Most prepare all-cellulose materials by uniaxial high pres- of the cohesion came from the small sides of the test sure thermocompression of cellulose. The effect of samples (parallel to the compression axis) and seemed moisture content (0–8 w/w%) and temperature mainly related to the entanglement of amorphized (175–250 C) was characterized through the mechan- cellulose at the interface between particles. Around ical properties (bending and tensile), morphology 200 C water accumulated and provoked delamination (scanning electron microscopy, X-ray tomography) upon pressure release, but at higher temperatures and microstructure (viscometric degree of polymer- water, in a subcritical state, may have been consumed ization, Raman spectroscopy, X-ray diffraction, solid- during the hydrolysis of amorphous 
TI - Cellulose consolidation under high-pressure and high-temperature uniaxial compression
JF - Cellulose
DO - 10.1007/s10570-019-02273-8
DA - 2019-01-28
UR - https://www.deepdyve.com/lp/springer-journals/cellulose-consolidation-under-high-pressure-and-high-temperature-hTP1eDjjWQ
SP - 2941
EP - 2954
VL - 26
IS - 5
DP - DeepDyve
ER -