TY - JOUR
AU - Hummert, C.
AB - A reliable, sensitive and selective multicomponent method has been developed to determine 12 differentFusarium mycotoxins (trichothecenes type A and B, zearalenone) simultaneously in cereal and grain samples using liquid chromatography tandem mass spectrometry (LC-ESI-MS/MS). The sample preparation based on a standard extraction step followed by two different kinds of solid phase clean-up (multifunctional MycoSep® material) for trichothecenes, and an immuno-affinity purification which combined antibodies for aflatoxins, ochratoxin A and zearalenone (AOZ-IAC). For quantification of zearalenone (ZON) an internal standard (zearalanone, ZAN) was used, whereas for trichothecenes a recovery standard (verrucarol, VOL) was applied. The average recoveries for the trichothecenes ranged from 65% for nivalenol (NIV) up to 96% for deoxynivalenol (DON) and 89% for zearalenone. The limit of quantification is different for each of the individual trichothecenes and in the range of 1 ppb to 10 ppb.
TI - A multicomponent method for Fusarium toxins in cereal based food and feed samples using HPLC-MS/MS
JO - Mycotoxin Research
DO - 10.1007/BF02954808
DA - 2008-09-13
UR - https://www.deepdyve.com/lp/springer-journals/a-multicomponent-method-for-fusarium-toxins-in-cereal-based-food-and-fAqVg56eF8
SP - 18
EP - 22
VL - 21
IS - 1
DP - DeepDyve
ER -