TY - JOUR
AU - Gere, Jeffrey, A.
AB - Abstract This communication describes a method for the solid phase extraction of phencyclidine (PCP) from urine, followed by GC/MS analysis. The method is linear over the range 5–1000 ng/mL and consistently produces cleaner chromatograms than can be obtained by liquid-liquid extraction. The limits of detection and quantitation are 0.47 and 1.38 ng/mL, respectively. Extraction efficiency, or recovery, was found to be 100.8 ± 6.5%, and the between-run precision was 3.5% (25 ng/mL, n = 51). This solid phase method for extraction of PCP from urine has several advantages over liquid-liquid extraction for laboratories of any size. * The opinions herein expressed are those of the authors and are not to be construed as those of the Department of the Army or the Department of Defense. This content is only available as a PDF. Author notes † Current address: National Institute on Drug Abuse, Rockville, MD. ** Current address: U.S. Army Medical Material Development Activity, Ft. Detrick, MD.
TI - Solid Phase Extraction of Phencyclidine from Urine Followed by Capillary Gas Chromatography/Mass Spectrometry
JF - Journal of Analytical Toxicology
DO - 10.1093/jat/16.5.337
DA - 1992-09-01
UR - https://www.deepdyve.com/lp/oxford-university-press/solid-phase-extraction-of-phencyclidine-from-urine-followed-by-MD3PqUABNU
SP - 337
EP - 339
VL - 16
IS - 5
DP - DeepDyve
ER -