TY - JOUR
AU1 - Ghayeni, Hamid Reza
AU2 - Razeghi, Reza
AU3 - Kazemi, Foad
AU4 - Olyaei, Abolfazl
AB - This article reports the nitration of Hydroxyl‐Terminated Polybutadiene (HTPB) backbone by facile and efficient “one pot” procedure, resulting in the formation of conjugated nitro‐alkene derivative of HTPB. The reaction was carried out with sodium nitrite and iodine. In order to optimization of the effective parameters on the synthesis of Nitro‐HTPB, the proportional amounts of reactant, amount of solvent and temperature were investigated and the effect of these parameters on the nitration double bond on HTPB backbone was evaluated. The product Nitro‐HTPB was characterized by FT‐IR, 1H NMR and 13C NMR spectroscopy as well as DSC, and TG.
TI - An Efficient Synthesis, Evaluation of Parameters and Characterization of Nitro‐Hydroxyl‐Terminated Polybutadiene (Nitro‐HTPB)
JF - Propellants, Explosives, Pyrotechnics
DO - 10.1002/prep.201700315
DA - 2018-01-01
UR - https://www.deepdyve.com/lp/wiley/an-efficient-synthesis-evaluation-of-parameters-and-characterization-5t9f0L3BeJ
SP - 574
EP - 582
VL - 43
IS - 6
DP - DeepDyve
ER -