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Crystal structure of 15-crown-5-trichlorobismuth, (C 10 H 20 O 5 )BiCl 3

Crystal structure of 15-crown-5-trichlorobismuth, (C 10 H 20 O 5 )BiCl 3 Zeitschrift für Kristallographie 207, 175 177 (1993) © by R. Oldenbourg Verlag, München 1993 0044-2968/93 $3.00 Crystal structure of 15-crown-5-trichlorobismuth, (C10H2o05)BiCl3 R. Weber, H. Kösters and G. Bergerhoff Institut für Anorganische Chemie der Universität Bonn, Gerhard-Domagk-Str. 1, D-53121 Bonn, Germany (Received November 30, 1992) C10 Source of material: ref. 1 see Orthorhombic, P2i2i2i (No. 19), a 7.70(1) Ä, b V= 1631.5 Á3, Z 4, R 0.096. = = 13.268(2) Á, c 15.972(7) A, 176 Table 1. Parameters used for the Diffractometer R. Weber, H. Kösters and G. Bergerhoff X-ray data collection Criterion for unobserved reflections: Number of refined Enraf-Nonius CAD4 Mo Ka radiation F0<4a(Fo) type: Wave length: (0.7107 Ä) 173 co/20 61.30 cm SHELX Crystal characteristics: colourless prisms, size 0.3 x 0.3 x 0.4 mm 293 K 36° parameters: Scan mode: li: Structure solution program used: Temperature of measurement: 20,, Number of unique reflections: Table 2. Final atomic coordinates and displacement parameters (in Atom Bi Á2) U12 U13 -0.0016(5 ) -0.019(4) 0.023(3 ) -0.012(4 ) 0.00(1) -0.03(1) -0.02(1) 0.00(1) -0.00(1) -0.03(5) -0.05(3) U¡so/U,i 0.0503(4) 0.121(6) 0.112(5 ) 0.127(6) 0.13(2) 0.17(2) 0.13(2) 0.13(2) 0.15(2) 0.4(1) U22 0.0395(3) 0.066(4) 0.095(5) 0.071(4) 0.11(1) 0.08(1) 0.08(1) 0.10(1) 0.14(2) 0.14(3) 0.08(2) 0.07(1) 0.10(2) http://www.deepdyve.com/assets/images/DeepDyve-Logo-lg.png Zeitschrift für Kristallographie - Crystalline Materials de Gruyter

Crystal structure of 15-crown-5-trichlorobismuth, (C 10 H 20 O 5 )BiCl 3

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Publisher
de Gruyter
Copyright
Copyright © 1993 by the
ISSN
2194-4946
eISSN
2196-7105
DOI
10.1524/zkri.1993.207.Part-1.175
Publisher site
See Article on Publisher Site

Abstract

Zeitschrift für Kristallographie 207, 175 177 (1993) © by R. Oldenbourg Verlag, München 1993 0044-2968/93 $3.00 Crystal structure of 15-crown-5-trichlorobismuth, (C10H2o05)BiCl3 R. Weber, H. Kösters and G. Bergerhoff Institut für Anorganische Chemie der Universität Bonn, Gerhard-Domagk-Str. 1, D-53121 Bonn, Germany (Received November 30, 1992) C10 Source of material: ref. 1 see Orthorhombic, P2i2i2i (No. 19), a 7.70(1) Ä, b V= 1631.5 Á3, Z 4, R 0.096. = = 13.268(2) Á, c 15.972(7) A, 176 Table 1. Parameters used for the Diffractometer R. Weber, H. Kösters and G. Bergerhoff X-ray data collection Criterion for unobserved reflections: Number of refined Enraf-Nonius CAD4 Mo Ka radiation F0<4a(Fo) type: Wave length: (0.7107 Ä) 173 co/20 61.30 cm SHELX Crystal characteristics: colourless prisms, size 0.3 x 0.3 x 0.4 mm 293 K 36° parameters: Scan mode: li: Structure solution program used: Temperature of measurement: 20,, Number of unique reflections: Table 2. Final atomic coordinates and displacement parameters (in Atom Bi Á2) U12 U13 -0.0016(5 ) -0.019(4) 0.023(3 ) -0.012(4 ) 0.00(1) -0.03(1) -0.02(1) 0.00(1) -0.00(1) -0.03(5) -0.05(3) U¡so/U,i 0.0503(4) 0.121(6) 0.112(5 ) 0.127(6) 0.13(2) 0.17(2) 0.13(2) 0.13(2) 0.15(2) 0.4(1) U22 0.0395(3) 0.066(4) 0.095(5) 0.071(4) 0.11(1) 0.08(1) 0.08(1) 0.10(1) 0.14(2) 0.14(3) 0.08(2) 0.07(1) 0.10(2)

Journal

Zeitschrift für Kristallographie - Crystalline Materials – de Gruyter

Published: Jan 1, 1993

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