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Zeitschrift für © by R. Kristallographie 203, 115-116 (1993) Oldenbourg Verlag, München 1993 0044-2968/93 $3,00 + 0.00 R. E. Gladyshevskii and E. Parthé Genève, 24 quai Ernest-Ansermet, Laboratoire de Cristallographie, Université de CH-1211 Geneva 4, Switzerland and O. L. Sologub and P. S. Salamakha 6 Lomonosova street, SU-290005 Department of Chemistry, L'viv University, (Received January 31, 1992) L'viv, Ukraine Source of material: Synthesis from the elements by arc melting and annealing at 800°C in evacuated quartz tubes. The structure is built up of intergrown A1B2-, BaAl4- and Cu3Au-type columns (see réf. 1). Tetragonal, P4/mbm (no 127), a 2, Rw 0.055. = = 12.9336(9), c 4.2596(6) Â, V 712.5(1) Â3, = = R. E. Gladyshevskii, E. Parthé, O. X-ray data collection L. Sologub and P. S. Salamakha Table 1. Parameters used for the Diffractometer type: Wave length: Philips PW1100 Mo characteristics : Temperature of measurement: Crystal (0.71073 Â) metallic (spheroid diameter 0.052 mm) 293 60° Ka radiation Number of unique reflections : 510 Criterion for unobserved reflections : F0 < Number of refined Scan mode: µ: Structure solution program used : 3cr(F0) parameters : 34 -2 546.04 cm"1 XTAL3.0 20m,,: Table 2. Final atomic coordinates and Atom displacement parameters
Zeitschrift für Kristallographie - Crystalline Materials – de Gruyter
Published: Jan 1, 1993
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