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Since emulsions tend to become unstable with increasing temperature, reactions in emulsions are usually not performed at high temperatures. We show that non-aqueous inverse miniemulsions are relatively stable at temperatures higher than 150 °C. As an example of this remarkable stability,...
Soluble and curable aromatic polyamides have great potential use as processable and heat-resistant polymeric materials. In this study, a novel series of soluble aromatic polyamides (CN-PPAs) containing phthalazinone moiety and crosslinkable terminal cyano groups were synthesized by...
Crosslinking junctions of vulcanized natural rubber were analyzed by solid-state NMR spectroscopy equipped with a field-gradient high speed magic angle spinning probe. Resolution of 1 H and 13 C NMR spectra and correlations between 1 H and 13 C of the vulcanized natural rubber were investigated...
New DPP-containing polyiminoarylenes were prepared from 1,4-diketo-2,5-dihexyl-3,6-di(4′-bromophenyl)pyrrolo(3,4- c )pyrrole and various arylamine derivatives using palladium-catalyzed amination reactions. The arylamine comonomers were aniline (ANI), t -butylaniline (TBA), 2-aminoanthracene...
In this study a nanocomposite monofilament composed of a nematic thermotropic liquid crystalline polymer (TLCP) mixed with 1.5 wt.% of carbon nanoparticles (CNP) was prepared by melt extrusion. The nanoparticles had either a fibrous (VGCF) or layered (GNP) geometry. The tensile strength and...
The influence of high energy ball milling process, HEBM, and the presence of TiO 2 nanoparticles on the non-isothermal crystallization and fusion behavior of the HDPE were investigated. HEBM was used to homogeneously disperse TiO 2 nanoparticles into a high density polyethylene, HDPE....
A new unsymmetrical and concoplanar aromatic diamine monomer containing trifluoromethyl and dimethyl groups, 3,5-dimethyl-4-(4-amino-2-trifluoromethylphenoxy)-4′-aminobenzophenone ( 3 ), was synthesized in a three-step reaction using 2,6-dimethylphenol and 4-nitrobenzoyl chloride as starting...
Rubber toughened polypropylene nanocomposites using two types of modified montmorillonite (organoclay) were explored with the objective of achieving an improved balance between stiffness and toughness. The effect of three blending sequences on microstructure and properties of the ternary...
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