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The results of investigations on thermal decomposition of NH 4 VO 3 in dry air have been presented. TG–DSC measurements were carried out under non-isothermal conditions at linear change of samples temperature in time and under isothermal conditions. Characterization of the products structure...
The oxidation, in a neat oxygen atmosphere, of high-purity and highly crystalline natural graphite and synthetic Kish graphite was investigated. The physico-geometric model function of the kinetic rate equation was experimentally determined by isothermal thermogravimetric analysis at 650 °C....
The information on heat of oxidation–reduction reactions is important for the heat balance and optimization of the autoclave design in the hydrometallurgical industry in ore processing. Pyrite (FeS 2 ) is a gangue mineral that presents with nickel-containing pentlandite, and copper-containing...
Ceramic–metal composites (cermets) containing 4 mol% yttria-zirconia (4YSZ) and Ni particles as anode materials in solid oxide fuel cells were prepared by two methods. The first method involves nickel oxalate dihydrate precipitation on the 4YSZ powder and decomposition at 360 °C in inert Ar...
The thermal decomposition kinetics of UO 2 C 2 O 4 ·3H 2 O were studied by TG method in a flowing nitrogen, air, and oxygen atmospheres. It is found that UO 2 C 2 O 4 ·3H 2 O decomposes to uranium oxides in four stages in all atmosphere. The first two stages are the same in the whole atmosphere...
In this study, the combustion kinetics of Göynük oil shale, polyethylene, polyethylene glycol (PEG), polymethyl methacrylate (PMMA), polyvinyl chloride, and polymer–oil shale blends were investigated by thermogravimetric analysis. Experiments were conducted at non-isothermal conditions with a...
Nickel ferrite powders were synthesized by thermal decomposition of the precursors obtained in the redox reaction between the mixture of Ni(NO 3 ) 2 ·6H 2 O and Fe(NO 3 ) 3 ·9H 2 O with polyalcohol: 1,4-butanediol, polyvinyl alcohol and also with their mixture. During this reaction the primary...
In this article, the effect of magnesium doping on the properties of bis(thiourea)zinc(II) chloride (BTZC) crystals has been described. The incorporation of Mg(II) into the crystal lattice was confirmed by energy dispersive X-ray spectroscopy and quantified by inductively coupled plasma...
Results from the measurement of the heat of reaction of hydrothermal carbonization by power compensated differential scanning calorimetry exhibited a comparably high experimental standard deviation of around 10–20%. The reasons for this standard deviation have been investigated and are being...
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