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Thermal decomposition of tetraethylammonium tetrachloro-, bromotrichloro-and tribromochloroferrates(III), of general formula ((C 2 H 5 ) 4 N)(FeBr 4−n Cl n ) ( n =1, 3, 4), has been studied using the TG-MS, DTA and DTG techniques. The measurements were carried out in an argon atmosphere over...
Inorganic pigments containing lanthanides based on pseudo cubic structure of SrSnO 3 have been prepared by solid state reaction between SrCO 3 , SnO 2 and lanthanide oxides (Tb 4 O 7 , Pr 6 O 11 , CeO 2 ) in the temperature range 1300–1550°C. The resultant materials were characterised by XRD,...
In this paper, a systematic analysis of the errors involved in the determination of the kinetic parameters (including the activation energy and frequency factor) from five integral methods has been carried out. The integral methods analyzed here are Coats-Redfern, Gorbachev,...
A calorimetric investigation on the reactions of TiCl 4 with phthalates in 1,1,2,2-tetrachloroethane (TCE) is presented in order to better understand the complex interactions present in Ziegler-Natta catalytic systems. The Lewis bases diethyl isophthalate ( L1 ), diethyl terephthalate ( L2 ) and...
4-Chloro-2-methoxybenzoates of heavy lanthanides(III) and yttrium(III) were obtained as mono-, di-, tri-or tetrahydrates with metal to ligand ratio of 1:3 and general formula Ln(C 8 H 6 ClO 3 ) 3 · n H 2 O, where n =1 for Ln =Er, n =2 for Ln =Tb, Dy, Tm, Y, n =3 for Ln =Ho and n =4 for Yb and...
In this work a commercially available organophilic Montmorillonite (Cloisite 30B) was modified by interaction with different surfactants, namely dodecylsuccinic anhydride (DSA), octadecylamine (ODA), octadecanoic alcohol (ODOH) and octadecanoic acid (ODAc), in order to increase its basal spacing...
Biogas generally contains significant quantities of carbon dioxide in addition to methane. A bubbling column reactor operating at atmospheric pressure is proposed for cheap separation and a Mettler RC1 reaction calorimeter was used to build a simplified empirical model for measuring the molar...
Thermokinetic parameters of the solid-state of poly( o -toluidine) (POT) doped with perchloric (HClO 4 ) acid was studied by thermogravimetric analysis (TG) and differential thermal analysis (DTA) under non-isothermal conditions. Molecular mechanics (MM) calculations suggest that the optimal...
Polyaniline/γ-Al 2 O 3 (PANI/γ-Al 2 O 3 ) composites were synthesized by in-situ polymerization at the presence of HCl as dopant by adding γ-Al 2 O 3 nanoparticles into aniline solution. The composites were characterized by FTIR and XRD. The thermogravimetry (TG) and modulated differential...
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