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Time and temperature resolved X-ray diffraction was used for thermal analysis. Series of diffraction patterns were measured, while the samples are heated/cooled stepwise or isothermally with freely selectable temperature programs. The method was applied for the investigation of the phase...
Glasses of composition expressed by the following general formula xCaO·(1−x)SiO 2 (0.30≤x≤0.50) can be prepared by means of the sol-gel route starting from tetramethylorthosilicate and calcium nitrate tetrahydrate They are all difficult to prepare by means of the traditional technique of...
Heat capacities (C p ) of solid benzene, biphenyl, p -terphenyl, p -quaterphenyl, and poly- p -phenylene were analyzed using the ATHAS Scheme of computation. The calculated heat capacities based on approximate vibrational spectra of solid benzene and the series of oligomers containing additional...
The thermal decomposition of poly(α,α,α′,α′-tetrafluoro- p -xylylene) (parylene AF-4) films with thicknesses of ca. 7.5 and 10 μm has been studied by both dynamic (10°C min −1 ) and isothermal TG in either nitrogen or oxygen atmospheres. In dynamic studies with nitrogen, gross...
Beypazari lignite was investigated by differential scanning calorimetry (DSC), thermogravimetry (TG), high pressure thermogravimetry (HPTG) and combustion cell experiments. All the experiments were conducted at non-isothermal heating conditions with a heating rate of 10°C min −1 , in the...
This work present comparative results on powder milk storage quality, obtained from analytical methods. Protein content was determined conventional (Kjeldahl) and colorimetric with biuret reagent at 540 nm and integral quality by thermogravimetric and biological methods. A method was developed...
A differential microcalorimeter (E. Calvet) was used to study the processes of adsorption of five aliphatic alcohols (C 1 -C 5 ) on α-Al 2 O 3 at 25, 50, 100, 150 and 200°C. In particular, the importance of the thermokinetic study of the chemisorption of such alcohols at different experimental...
The local anesthetic drug tetracaine hydrochloride is described in the Europ. Pharmacopea with a melting point of 148°C or with a range of 134 to 147°C due to the melting points of two other forms. The polymorphic behaviour of tetracaine hydrochloride has been studied by using thermal...
DSC can be used to quickly determine if a product labeled as butter is actually a recombined butter made without milk. Recombined butter is manufactured from anhydrous milk fat, skim milk powder, water, salt, and lecithin. Melting profiles of tempered samples of natural butter and recombined...
ADSC with its periodical temperature programs combines the features of DSC measured at high heating rate (high sensitivity) with those at low heating rate (high temperature resolution). In addition, the “reversing” c p effects can be separated from the “non-reversing” latent heat effects....
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