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10.1002/jps.2600630222.abs A method is presented for the quantitative analysis of sodium o‐iodohippurate by high‐speed liquid chromatography. Following a preliminary extraction to remove benzyl alcohol, the samples are acidified and extracted with ethyl acetate. After evaporation of the...
10.1002/jps.2600630211.abs Electric dipole moments of nine N, N‐dimethylaniline derivatives were determined experimentally in benzene solution according to literature methods. The theoretical dipole moments of these compounds were calculated from molecular orbital approximations according to...
10.1002/jps.2600630218.abs Twenty‐five N‐substituted N′‐cyano‐O‐(triorganostannyl)isoureas were synthesized by the reaction of (triphenylstannyl)cyanamide or (trimethylstannyl)cyanamide with various organic isocyanates. The IR spectrum of each compound was obtained over the 4000–30...
10.1002/jps.2600630209.abs The presence of a stereospecific soluble esterase that hydrolyzes the three forms of oxazepam succinate half‐ester ((+), (−), and (±)) in some tissues of rats, mice, and guinea pigs was demonstrated. The enzymatic activity was determined by a titrimetric method....
10.1002/jps.2600630224.abs Microencapsulation of solid stearyl alcohol particles by complex coacervation was studied. Spherical particles of solid stearyl alcohol were prepared by the vibrating capillary method. Various size fractions of these particles were encapsulated by a modified technique...
10.1002/jps.2600630227.abs 5‐Acetamido‐1‐methyl‐2‐(2′‐pyrimidyl)imidazole is shown to be one metabolite of 1‐methyl‐5‐nitro‐2‐(2′‐pyrimidyl)imidazole in both rats and humans. Characterization was carried out by mass spectroscopy, NMR, and IR and by synthesis of the...
10.1002/jps.2600630212.abs Since estimates in the literature for the fundamental binding parameters of dicumarol to bovine serum albumin show wide disparity, these phenomena were reinvestigated, using a nonequilibrium partitioning technique. A three‐phase system was used consisting of an...
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