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10.1002/jps.2600530322.abs Purity determined by solubility analysis was used to evaluate the efficacy of other analytical methods for measuring thermal degradation. Techniques for filtration and a method for calculation of confidence interval for solubility analysis are described.
10.1002/jps.2600530306.abs Columbianadin and columbianin were isolated from petroleum ether and alcoholic extracts, respectively, of Lomatium columbianum. Upon hydrolysis, these coumarins yielded tiglic acid and glucose, respectively, and an alcohol, columbianetin. This alcohol was dehydrated to...
10.1002/jps.2600530315.abs A single step process for the production of tablet granulations on a continuous basis is described. The process is based on the use of a modified fluidized bed dryer. Important considerations in the design and operation of the equipment are derived from material and...
10.1002/jps.2600530305.abs 3‐(γ‐Aminopropyl)‐5‐ethoxyindole has been synthesized from p‐phenetidine and α‐methylacetoacetate. This method involves fewer intermediates, with new and better methods for their purification.
10.1002/jps.2600530319.abs The effect of the trifluoromethyl group on the biological properties of four new isomeric (trifluoromethyl) phenylmercuric chlorides was evaluated with a representative strain of Micrococcus pyogenes (var. aureus) using the Vincent paper disk modification of the Oxford...
10.1002/jps.2600530304.abs The total body potassium in humans was determined by measuring the K40 radioactivity in a whole body liquid scintillation counter. These values were used to study the lean body mass and the fat content as a function of age and physical fitness. The effect of an...
10.1002/jps.2600530316.abs Data collected from batch runs in a 1‐ft. diameter fluidized bed granulator were employed in preliminary evaluation of process performance. Moisture content, granule screen analysis, and compressibility tests were used to evaluate the granulated product. Process...
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