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The voltammetric response of per-cathodic activated carbon steel electrode in deaerated 0.50 m NaHCO 3 solution at pH 8.72 and 25 °C at a scan rate of 25 mV s −1 was investigated. The influence of cycling, potential excursion and scanning rate on the anodic behavior was studied. The results...
Interest in copper as a technologically important material needs to be met with greater understanding of the fundamental chemical reactions of copper. In particular, there is still a lack of universal agreement on the oxidation process of bulk copper and thin copper films. In this study, the...
Characterisation of a direct methanol fuel cell using an anode fabricated by thermal decomposition from Pt–Ru chloro-complex on Ti mesh is described. The polarisation characteristic of the resultant membrane electrode assembly is compared with that of a conventional MEA with an anode,...
NO decomposition in solid electrolyte cells was investigated in the presence of excess O 2 . The results show that NO is decomposed via an electrocatalytic mechanism rather than electrolysis in the range of 1–4 V of applied voltage. The NO is catalytically decomposed to N 2 on the cathode...
Direct cathodic reduction of dyes which contain an azo-goup in the chromophore was successfully used for decolourisation of intensively coloured concentrates from Nanofiltration treatment of textile effluents. Based on laboratory scale experiments, a technical multi-cathode electrolyser was...
The deposition of manganese oxide on a carbon substrate in manganese acetate solution by anodic deposition was investigated. The effects of electrolyte concentration (0.05–1 m) and temperature (0–50 °C) on the characteristics of the oxide prepared were explored. The surface morphology of the...
A study has been made of the electrochemical etching of 99.99% aluminum foils at a current density of 50 mA cm −2 in AlCl 3 –HCl solutions (1 m Cl − ) at 80 °C. The solutions were made by dissolving metallic aluminum into 1m HCl solution, to give a Cl − concentration of 1 m. The number...
Open-circuit potential, polarization and electrochemical impedance spectroscopy (EIS) measurements were used to investigate the corrosion behaviour of Ti–6Al–4V alloy in H 2 SO 4 and HCl solutions. The corrosion rate of the alloy was found to increase with increasing acid concentration. The...
Polybithiophene (PBT) was freshly electrodeposited on platinum (Pt) and steel electrodes using cyclic voltammetry from 2,2′-bithiophene (BT), electrolyte and acetonitrile (AC). The electrolytes used were LiBF 4 , LiClO 4 , LiCF 3 SO 3 , Bu 4 NBF 4 , Bu 4 NClO 4 , or Bu 4 NCF 3 SO 3 . Black to...
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