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Electrowinning of zinc from zinc chloride solutions, acidified by HCl, was conducted in a cation exchange membrane cell. The current efficiency was correlated with the deposit morphology. The deposits having lesser surface defects, which act as active sites for hydrogen adsorption, exhibited...
Cyclic voltammetry studies were carried out on a platinum electrode in alkaline 1 M NaOH solutions containing 0.1 M of phenol, monochlorophenols, dichlorophenols, trichlorophenols and pentachlorophenol in order to compare their electropolymerization ability and the degree of deactivation of the...
The corrosion of Au–Pd–In alloy, which is of great importance in dentistry, has been studied using an electrochemical quartz crystal microbalance (EQCM) in simulated physiological solutions. The alloy was deposited on quartz substrates by means of magnetron sputtering (MS). Analysis performed...
Optimal conditions for Sn and Co codeposition were achieved in slightly acid citrate solutions containing no excess of ligand. Sn–Co coatings were deposited with amounts of Co ranging from 15 to 86 mass %. Bright deposits were obtained when the Co content exceeded 76%. These coatings may be...
The removal of nickel ions from a low cross-linked ion-exchange resin using an applied electrical potential gradient was studied. The potential gradient across a bed of ion-exchange particles, in which nickel ions were absorbed, was varied by two methods. One involved a change of cell voltage...
Novel solid films of a mixed polynuclear hexacyano iron(III) and decavanadates have been electrochemically prepared. The colour of these solid thin films ranged from yellow to blue depending on the thickness. The cyclic voltammograms (CVs) of these solid films indicate the involvement of both...
The redox behaviour of copper species in an 'ammonium imide' room temperature molten salt was examined to clarify the applicability of the salt to the electroplating media of various metals. Trimethyl- n -hexylammonium bis((trifluoromethyl)sulfonyl)amide (TMHA-Tf 2 N), having an electrochemical...
A new Se-doped spinel material, LiAl 0.18 Se 0.02 Mn 1.8 O 4 powder with a phase-pure polycrystalline was synthesized by a sol–gel method. The material in the 3 V region (2.4 ∼ 3.5 V) and both the 3 and 4 V region (2.4 ∼ 4.4 V) initially deliver a discharge capacity of 81 and 178 mA h g...
Molten copper containing variable quantities of oxygen up to the saturation concentration 0.8 wt % O can be effectively deoxidized by calcium chloride melts containing 5 wt % calcium carbide. Cyclic voltammetry, on solid copper electrodes in this melt at a temperature of 1073 K, revealed the...
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