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A method has been developed to produce composition modulated Bi 1− x Sb x alloys by electrodeposition. The electrolyte which consists of NaCl 4 M and HCl 1 M (pH 0) in aqueous medium, allows codeposition of bismuth and antimony to be accomplished at room temperature on glassy carbon. The...
We describe and implement a microelectrode procedure for the determination of important transport properties required for the evaluation of liquid electrolytes used in lithium-based batteries. Three solvents of interest (propylene carbonate, ethylene carbonate, and diethyl carbonate) and two...
Comparative results of electrochemical investigations of polymeric composites with different contents of carbon black and graphite activated with ruthenium oxides are presented. Electrochemical impedance measurements (EIS), enabling determination of electrical and electrochemical properties of...
The effect of benzotriazole, BTA, on mass transfer in dissolution-corrosion of the copper rotating disk electrode in 0.02 M Fe(III)–0.5 M H 2 SO 4 has been studied by means of atomic absorption spectrometry. The mass transfer coefficient, K , was determined from the slope of ln( C 0 / C )...
The anodic behaviour of four cast iron alloys containing up to 16.7% Ni, in deaerated 60 wt% H 3 PO 4 with and without 5 × 10 −3 M F − , Cl − ions and 1:1 Cl − /F − mixture was studied by the potentiostatic technique. Values of E corr of the alloys are markedly influenced by their...
Anodes for the electrocatalytic oxidation of organic pollutants in water have been prepared by depositing novel Sb-doped SnO 2 material on Ti supports by the sol–gel technique. Surface analysis of the anodes by nuclear microprobe and XPS-measurements confirmed the formation of a doped film on...
The stannous ion consumption in methane sulfonic acid (MSA) baths with and without catechol was quantitatively evaluated using platinum and IrO 2 –Ta 2 O 5 /Ti anodes. The stannous ion is consumed at the same rate with both anodes, accompanied by the generation of tin sludge on the anode...
Alternating current impedance data of alkaline Zn/MnO 2 cells were analysed in view of identification of suitable parameters, which depend on the state-of-charge (SOC) of the cells. The impedance of a slightly discharged cell was found to possess impedance considerably lesser than that of an...
Electrochemical studies on AB 2 type Zr 0.5 Ti 0.5 V 0.6 Cr 0.2 Ni 1.2 metal hydride electrodes with varying particle size suggests that the electrodes with alloy particles of about 60 μm yield the optimum performance. The values for diffusion coefficient of hydrogen in the alloy particles > 25...
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