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Experiments were performed using a microparticle image velocimetry (MPIV) for 2D velocity distributions of electroosmotically driven flows in a 40-mm-long microchannel with a square cross section of 200×200 μm. Electroosmotic flow (EOF) bulk fluid velocity measurements were made in a range of...
We review recent structural investigations done by anomalous small-angle X-ray scattering (ASAXS). ASAXS uses the dependence of the scattering length of a given element if the energy of the incident X-ray beam is near the absorption edge of this element. The analysis of the ASAXS data leads to...
Water-soluble, amphiphilic diblock copolymers were synthesized by reversible addition fragmentation chain transfer polymerization. They consist of poly(butyl acrylate) as hydrophobic block with a low glass transition temperature and three different nonionic water-soluble blocks, namely, the...
A novel technique to estimate the distribution state of carboxyl groups within submicron-sized, carboxylated polymer particles was proposed. For the purpose, carboxyl groups in two kinds of butyl methacrylate–methacrylic acid copolymer emulsion, which were prepared by emulsion copolymerizations...
The formation and the optical features of two-dimensional aggregates formed by DNA-directed immobilization and cross-linking of bifunctional DNA–gold nanoparticles at flat gold substrates are analyzed. The samples are structurally characterized by atomic force microscopy to evaluate the...
Low shear rate and low frequency measurements focused on the extremely slow dynamics of a three-dimensional body-centered cubic (BCC) structure of an asymmetric block copolymer under nanophase-separated conditions. The material studied was poly(styrene- b -ethylene- co -butylene- b -styrene)...
Optical tweezers are microscopic tools with extraordinary precision in the determination of the position (±2 nm) of a colloid (diameter: ∼2.0 μm) in 3D-space and in the measurement of small forces in the range between 0.1 and 100 pN (pN=10 −12 N). Experiments are reported in which single...
The preparation of carboxylated hyperbranched polyglycerols of narrow polydispersity was achieved by modification (78–90%) of the hydroxyl end groups via Michael addition of acrylonitrile, followed by hydrolysis. High conversion could only be achieved for low molecular weight starting materials...
Thermoresponsive colloidal particles were prepared by seeded precipitation polymerization of N -isopropylacrylamide (NIPAM) in the presence of a crosslinking monomer, N , N -methylenebisacrylamide (MBA), using polystyrene latex particles (ca. 50 nm in diameter) as seeds in aqueous dispersion....
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