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The mild title method provides various N,2‐diarylacetamides in moderate to often high yields.
A benzannulation of [5‐(phenylthio)pent‐4‐enyl]pyridinylacetylenes yields cyclopentaisoquinolines via a cascade process.
The key step in the synthesis of the entitled compounds (IV) is an extraordinary Wittig reaction of phenanthrene‐9,10‐dione (I) and two equivalents of benzylidenetriphenylphosphoranes (II) followed by a dehydrogenation step using DDQ.
The simple method proceeds under mild and metal‐free reaction conditions in an environmentally benign solvent.
Review: 48 refs.
A novel in situ synthesis of dichlorotriphenylphosphorane is accomplished upon combining triphenylphosphine and the hypervalent iodine reagent iodobenzene dichloride.
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