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The title compound, C18H18Cl2N2O2, was synthesized by the reaction of 1-(5-chloro-2-methoxyphenyl)ethanone with hydrazine hydrate. The molecule lies on a crystallographic twofold axis passing through the mid-point of the N-N bond with one half-molecule in the asymmetric unit. The dihedral angle...
The title compound, C18H12N2, adopts an E conformation with the benzylidenemalononitrile and phenyl groups located on opposite sides of the C=C bond. The two phenyl rings are oriented at a dihedral angle of 62.49 (7)Degrees.
In the structure of the title compound, Mo(C11H13NO3)O2(CH3OH), the MoVI ion is octahedrally coordinated by two oxide O atoms, the N atom and two deprotonated OH groups of the tridentate Schiff base ligand 2-methoxy-6-(2-oxidopropyl)iminomethylphenolate and by a methanol O atom. In the crystal...
In the title compound, C6H7BrN+.C6H2N3O7-, the O atoms of two of the nitro groups are disordered over two sites, the ratios of the refined occupancies being 0.72 (6):0.28 (6) and 0.74 (5):0.26 (5). In the crystal structure, the anions and cations are linked via intermolecular N-HO hydrogen bonds...
In the cation of the title compound, CoCl(C10H8N2)2ClO4, the CoII atom displays a distorted trigonal-bipyramidal coordination geometry. The two pyridine rings in each 2,2'-bipyridine ligand form dihedral angles of 10.75 (12) and 4.28 (13)Degrees. The crystal packing is stabilized by interionic...
The title compound, Au(C9H9ClNOS)(C18H15P), reveals a near linear geometry for the Au atom defined by a S,P-donor set S-Au-P = 175.86 (3)Degrees. The deviation from linearity is ascribed to the proximate O atom derived from the thiocarbamato anion AuO = 2.967 (3) A.
The title compound, C9H7ClN2O2, was prepared by reaction of methyl 4-chloro-3-(prop-1-ynyl)picolinate with hydroxylamine in MeOH/KOH solution. The two essentially planar molecules which make up the asymmetric unit have almost identical geometries and and are linked into dimeric aggregates via...
In the title compound, K+.C14H9O4S2-.C14H10O4S2, the hydrogen 2,2'-dithiodibenzoate and 2,2'-disulfanediyldibenzoic acid species combine to provide an O6S2 donor set to the potassium cation based on a cubic geometry. KS 3.1733 (7) and 3.5499 (8) A and KO 2.6586 (16)-3.0661 (15) A) interactions,...
The asymmetric unit of the title complex, PdI2(C10H8N2), contains one half of the formula unit. The Pd2+ ion is located on a twofold rotation axis and is four-coordinated in a slightly distorted square-planar environment by two N atoms of the chelating 2,2'-bipyridine ligand and two iodide ions....
The 3,5-methoxy groups in the title compound, C16H23NO4, are almost coplanar with the aromatic ring, whereas the 4-methoxy group is bent out of this plane. The three CH3-O-C-C torsion angles are -1.51 (18), 0.73 (19) and 75.33 (15)Degrees. The cyclohexane ring adopts a chair conformation. In the...
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