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The title compound, C18H18Cl2N2O2, was synthesized by the reaction of 1-(5-chloro-2-methoxyphenyl)ethanone with hydrazine hydrate. The molecule lies on a crystallographic twofold axis passing through the mid-point of the N-N bond with one half-molecule in the asymmetric unit. The dihedral angle...
The title compound, C18H12N2, adopts an E conformation with the benzylidenemalononitrile and phenyl groups located on opposite sides of the C=C bond. The two phenyl rings are oriented at a dihedral angle of 62.49 (7)Degrees.
In the cation of the title compound, CoCl(C10H8N2)2ClO4, the CoII atom displays a distorted trigonal-bipyramidal coordination geometry. The two pyridine rings in each 2,2'-bipyridine ligand form dihedral angles of 10.75 (12) and 4.28 (13)Degrees. The crystal packing is stabilized by interionic...
In the structure of the title compound, Mo(C11H13NO3)O2(CH3OH), the MoVI ion is octahedrally coordinated by two oxide O atoms, the N atom and two deprotonated OH groups of the tridentate Schiff base ligand 2-methoxy-6-(2-oxidopropyl)iminomethylphenolate and by a methanol O atom. In the crystal...
In the title compound, C6H7BrN+.C6H2N3O7-, the O atoms of two of the nitro groups are disordered over two sites, the ratios of the refined occupancies being 0.72 (6):0.28 (6) and 0.74 (5):0.26 (5). In the crystal structure, the anions and cations are linked via intermolecular N-HO hydrogen bonds...
The title compound, Au(C9H9ClNOS)(C18H15P), reveals a near linear geometry for the Au atom defined by a S,P-donor set S-Au-P = 175.86 (3)Degrees. The deviation from linearity is ascribed to the proximate O atom derived from the thiocarbamato anion AuO = 2.967 (3) A.
The title compound, C9H7ClN2O2, was prepared by reaction of methyl 4-chloro-3-(prop-1-ynyl)picolinate with hydroxylamine in MeOH/KOH solution. The two essentially planar molecules which make up the asymmetric unit have almost identical geometries and and are linked into dimeric aggregates via...
In the title compound, K+.C14H9O4S2-.C14H10O4S2, the hydrogen 2,2'-dithiodibenzoate and 2,2'-disulfanediyldibenzoic acid species combine to provide an O6S2 donor set to the potassium cation based on a cubic geometry. KS 3.1733 (7) and 3.5499 (8) A and KO 2.6586 (16)-3.0661 (15) A) interactions,...
The asymmetric unit of the title complex, PdI2(C10H8N2), contains one half of the formula unit. The Pd2+ ion is located on a twofold rotation axis and is four-coordinated in a slightly distorted square-planar environment by two N atoms of the chelating 2,2'-bipyridine ligand and two iodide ions....
The 3,5-methoxy groups in the title compound, C16H23NO4, are almost coplanar with the aromatic ring, whereas the 4-methoxy group is bent out of this plane. The three CH3-O-C-C torsion angles are -1.51 (18), 0.73 (19) and 75.33 (15)Degrees. The cyclohexane ring adopts a chair conformation. In the...
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