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References (7)
-
Z. Gu, S. Zhang, C. Wang, W. Lian, P. Xiao, J. Chen (1997)
[Determation of strychnine and brucine in Strychnos by HPLC].Yao xue xue bao = Acta pharmaceutica Sinica, 32 10
-
Y. Choi, Y. Sohn, C. Kim, K. Oh, Jinwoong Kim (2004)
Analysis of strychnine from detoxified Strychno nux-vomica seeds using liquid chromatography–electrospray mass spectrometryJournal of Ethnopharmacology, 93
-
Zhongxi Li, Yue Guo (2005)
Simultaneous determination of trace arsenic, antimony, bismuth and selenium in biological samples by hydride generation-four-channel atomic fluorescence spectrometry.Talanta, 65 5
-
Yuqin Li, Shengda Qi, Xingguo Chen, Zhide Hu (2004)
Separation and determination of the anthraquinones in Xanthophytum attopvensis pierre by nonaqueous capillary electrophoresis.Talanta, 65 1
-
Hua‐tao Feng, Sam Li (2002)
Determination of five toxic alkaloids in two common herbal medicines with capillary electrophoresis.Journal of chromatography. A, 973 1-2
-
Hua‐tao Feng, Lingling Yuan, Sam Li (2003)
Analysis of Chinese medicine preparations by capillary electrophoresis-mass spectrometry.Journal of chromatography. A, 1014 1-2
-
Charlotte Duverneuil, G. Grandmaison, P. Mazancourt, J. Alvarez (2004)
Liquid chromatography/photodiode array detection for determination of strychnine in blood: a fatal case report.Forensic science international, 141 1
- Publisher
- Springer Journals
- Copyright
- Copyright © 2006 by Friedr. Vieweg & Sohn/GWV Fachverlage GmbH
- Subject
- Chemistry; Chromatography; Proteomics; Pharmacy; Laboratory Medicine
- ISSN
- 0009-5893
- eISSN
- 1612-1112
- DOI
- 10.1365/s10337-006-0734-9
- Publisher site
- See Article on Publisher Site
Abstract
A nonaqueous capillary electrophoresis method with photo diode-array detection was developed for the analysis of strychnine and brucine in Strychnos nux-vomica L. The separation of the two alkaloids was optimized with respect to the concentration of Tris-boric acid, the proportion of methanol and acetonitrile, and applied voltage. Baseline separation was obtained for the two analytes within 10 min using a running buffer containing 25 mM Tris-boric acid, 60% methanol and 20% acetonitrile with acetic acid adjusting pH to 4.0. In this paper, the method was used to determine the contents of strychnine and brucine in raw material and prepared Strychnos nux-vomica L.
Journal
Chromatographia – Springer Journals
Published: Feb 28, 2006