Get 20M+ Full-Text Papers For Less Than $1.50/day. Start a 14-Day Trial for You or Your Team.

Learn More →

Chromatographic separation and quantitative determination of metal ions in wool material

Chromatographic separation and quantitative determination of metal ions in wool material Quantitative determination of iron, copper and manganese in woollen material by means of thin layer chromatography is described. The fabric sample was combusted and the residue dissolved in HCl (1∶1). The optimal separation on cellulose was achieved with the solvent system ethanol+1-butanol+HCl+H 2 O (60∶30∶5∶5, v/v). Locating reagent was sodium diethyldithiocarbaminate (used as 5% ethanol solution). It was found that in woollen cloth iron, copper and manganese could be detected down to 20 μg per gram of material. http://www.deepdyve.com/assets/images/DeepDyve-Logo-lg.png Chromatographia Springer Journals

Chromatographic separation and quantitative determination of metal ions in wool material

Loading next page...
 
/lp/springer-journals/chromatographic-separation-and-quantitative-determination-of-metal-kQ0U2uoNSH

References (4)

Publisher
Springer Journals
Copyright
Copyright © 1992 by Friedr. Vieweg & Sohn Verlagsgesellschaft mbH
Subject
Chemistry; Analytical Chemistry; Organic Chemistry; Biochemistry, general; Plant Sciences; Pharmacy; Measurement Science, Instrumentation
ISSN
0009-5893
eISSN
1612-1112
DOI
10.1007/BF02269878
Publisher site
See Article on Publisher Site

Abstract

Quantitative determination of iron, copper and manganese in woollen material by means of thin layer chromatography is described. The fabric sample was combusted and the residue dissolved in HCl (1∶1). The optimal separation on cellulose was achieved with the solvent system ethanol+1-butanol+HCl+H 2 O (60∶30∶5∶5, v/v). Locating reagent was sodium diethyldithiocarbaminate (used as 5% ethanol solution). It was found that in woollen cloth iron, copper and manganese could be detected down to 20 μg per gram of material.

Journal

ChromatographiaSpringer Journals

Published: Dec 1, 1992

There are no references for this article.