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W. Buchmann, B. Desmaziéres, J. Morizur, H. Nguyen, H. Chéradame (2000)
Synthesis of Polymers Containing Pseudohalide Groups by Cationic Polymerization. 16.† Model Reactions and Oligomerization of Isobutylene with 2-Isothiocyanato-2-phenylpropane/TiCl4 as Initiating SystemMacromolecules, 33
E. Bach, A. Kjær, R. Shapiro, C. Djerassi, E. Pedersen, J. Nielsen (1965)
Mass Spectra of two Deuterated Isothiocyanates.Acta Chemica Scandinavica, 19
H. Budzikiewicz, C. Djerassi, Dudley Williams (1967)
Mass spectrometry of organic compounds
J. Kennedy, B. Iván (1992)
Designed Polymers by Carbocationic Macromolecular Engineering
A. Kjær, M. Ohashi, J. Wilson, C. Djerassi, J. Munch‐Petersen (1963)
Mass Spectra of Isothiocyanates.Acta Chemica Scandinavica, 17
An analytical strategy has been developed for analysis of polyisobutylenes partially functionalized with isothiocyanate groups ( $$\bar M_n< 2000g mol^{ - 1} $$ ) by capillary supercritical-fluid chromatography (CSFC), size- exclusion chromatography (SEC), and reversed-phase liquid chromatography (RPLC). Fractions collected from semi-preparative RPLC and SEC were further characterized by capillary GC-MS (gas chromatography coupled with mass spectrometry). Complete characterization of the polymer was achieved by comparing the results obtained from the different techniques. The degree of polymerization and the relative quantity of the different series of macromolecular chains of polyisobutylene were estimated.
Chromatographia – Springer Journals
Published: Aug 28, 2006
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