Absolute configuration of two bases co-crystallized with (+)-tartaric acid: (R)-1-3-(4-chlorophenyl)-3-hydroxy-3-(2-pyridyl)propylpyrrolidinium (+)-tartrate 2-propanol hemihydrate and (S)-2-1-hydroxy-1-(4-methoxyphenyl)ethylpyridinium (+)-tartrate
Abstract
<h2>Acta Crystallographica Section C</h2><h3>Crystal Structure Communications</h3><h3>0108-2701</h3> <h2>research papers (organic compounds)</h2> Volume 47 Part 8 Pages 1645-1649 August 1991 <h2>Absolute configuration of two bases co-crystallized with (+)-tartaric acid: ( R )-1-[3-(4-chlorophenyl)-3-hydroxy-3-(2-pyridyl)propyl]pyrrolidinium (+)-tartrate 2-propanol hemihydrate and ( S )-2-[1-hydroxy-1-(4-methoxyphenyl)ethyl]pyridinium (+)-tartrate</h2> B. Kojic-Prodic, Z. Ruzic-Toros and N. Bresciani-Pahor Acta Cryst. (1991). C47, 1645-1649 Absolute Configuration of Two Bases Co-crystallized with (+)-Tartaric Acid: (R)-l-[3-(4-Chlorophenyl)-3-hydroxy-3-(2-pyridyl)propyllpyrrolidinium ( + )-Tartrate 2-Propanol Hemihydrate and (S)-2-[1-Hydroxy-l-(4-methoxyphenyl)ethyllpyridinium ( + )-Tartrate BY BISERKA KOJI~-PRODI6* AND 7,IVA RU~Idz-TORO~ Rudjer Bos~kovid Institute, POB 1016, 41001 Zagreb, Yugoslavia AND NEVENKA BRESCIANI-PAHOR Universitd degli Studi di Trieste, Dipartimento di Scienze Chimiche, Piazzale Europa 1, 34127 Trieste, Italy (Received 3 July 1990; accepted 14 January 1991) Abstract. (1) C18H22C 1N20 + .C4H506-- .C3H80. ~H20, Mr= 536"08, monoclinic, P2~, a= 13.738 (3), b = 15.037(5), c=7.012(2) A, fl=103.26(2)°, V= 1409.9 (5)/~3, Z = 2, Dx = 1.260 Mg m-3, ,~(Mo Ka) = 0.71069 ,~, /z = 0.181 mm-1, F(000) = 570, T = 295 K, R = 0.041, wR = 0.047 for 1606 reflections [I > 3o,(/)]. (2) CI4Hi6NOf.C4HsO6, Mr=379'37, monoclinic, ;~,1a= 16.036 (2),b= 7.839 ~2),c= 7.548 (1) ,~, 02.97 (1)°, V= 924.6 (5) A Z= 2, Dx = 1.367 Mg m-3, A(Mo Ka) =