2,2'-Iminobis(acetamide oxime)
Abstract
<h2>Acta Crystallographica Section B</h2><h3>Structural Crystallography and Crystal Chemistry</h3><h3>0567-7408</h3> <h2>short structural papers</h2> Volume 36 Part 12 Pages 3121-3123 December 1980 <h2>2,2'-Iminobis(acetamide oxime)</h2> X. Solans, C. Miravitlles, J. P. Declercq and G. Germain Acta Cryst. (1980). B36, 3121-3123 3121 2,2'-Iminobis(aeetamide oxime) BY X. SOLANS AND C. MIRAVITLLES Departamento de Cristalograf{a y Mineralog:a, Universidad de Barcelona, Granv:a 585, Barcelona 7, Spain and UEI de Difraeeidn de Rayos X y Estrueturas Cristalinas del Instituto 'Jaime Almera' del CSIC, Egipciacas 11, Barcelona 1, Spain AND J. P. DECLERCQ AND G. GERMAIN Laboratoire de Chimie Physique et de Cristallographie, Universitd de Louvain, 1 place Louis Pasteur, B- 1348 Louvain-la-Neuve, Belgium (Received 24 July 1979; accepted 14 May 1980) Abstract. C4HI1NsO2, Mr = 161.16, F(000) = 344, monoclinic, P2~/a, a = 10.458 (4), b -- 11.388 (4), c = 6.208 (2) A,B= 102.22(3)°, V= 722.6 (6) A3, Z = 4, D,, = 1.53 (2) (pycnometer), Dc = 1.48 Mg m-3, 2 (Cu Ka) = 1.54178 A. The structure was solved using MULTAN and refined by the block-diagonal least- squares method. The final R value is 0.061 for 1129 observed reflections. The C-C torsion angles between the N(amine) and the N(oxime) atoms are -30.5 (5) and